 
       
     
    
      AI10382-GC-MS-Food Safety-Analysis - page 77
      
              
          Dimethomorph
        
        
          0-200
        
        
          0.9995
        
        
          37
        
        
          0.9996
        
        
          181
        
        
          0.9984
        
        
          42
        
        
          Diphenylamine
        
        
          0-200
        
        
          0.9999
        
        
          12
        
        
          0.9994
        
        
          24
        
        
          0.9969
        
        
          22
        
        
          Endosulfan
        
        
          0-1000
        
        
          0.9994
        
        
          7
        
        
          0.9961
        
        
          4
        
        
          0.9969
        
        
          17
        
        
          Endosulfan sulfate
        
        
          0-200
        
        
          0.9988
        
        
          4
        
        
          0.9920
        
        
          2
        
        
          0.9980
        
        
          20
        
        
          EPN
        
        
          0-200
        
        
          0.9960
        
        
          2
        
        
          0.9947
        
        
          56
        
        
          0.9926
        
        
          0
        
        
          Epoxiconazole
        
        
          0-200
        
        
          0.9992
        
        
          5
        
        
          0.9966
        
        
          14
        
        
          0.9994
        
        
          8
        
        
          Ethion
        
        
          0-200
        
        
          0.9977
        
        
          11
        
        
          0.9967
        
        
          21
        
        
          0.9995
        
        
          3
        
        
          Ethoprop (Ethoprophos)
        
        
          0-200
        
        
          0.9998
        
        
          7
        
        
          0.9997
        
        
          16
        
        
          0.9978
        
        
          17
        
        
          Etofenprox
        
        
          0-200
        
        
          0.9985
        
        
          15
        
        
          0.9939
        
        
          60
        
        
          0.9986
        
        
          3
        
        
          Fenamiphos
        
        
          0-200
        
        
          0.9996
        
        
          2
        
        
          0.9992
        
        
          40
        
        
          0.9999
        
        
          41
        
        
          Fenamiphos sulfone
        
        
          0-200
        
        
          0.9968
        
        
          16
        
        
          0.9981
        
        
          74
        
        
          0.9933
        
        
          25
        
        
          Fenamiphos-sulfoxid
        
        
          0-2000 0.9907
        
        
          10
        
        
          0.9940
        
        
          101
        
        
          0.8709
        
        
          44
        
        
          Fenarimol
        
        
          0-200
        
        
          0.9979
        
        
          2
        
        
          0.9958
        
        
          8
        
        
          0.9987
        
        
          22
        
        
          Fenbuconazol
        
        
          0-200
        
        
          0.9990
        
        
          7
        
        
          0.9949
        
        
          33
        
        
          0.9991
        
        
          6
        
        
          Fenitrothion
        
        
          0-200
        
        
          0.9994
        
        
          15
        
        
          0.9993
        
        
          15
        
        
          0.9992
        
        
          23
        
        
          Fenoxycarb
        
        
          0-200
        
        
          0.9990
        
        
          9
        
        
          0.9970
        
        
          52
        
        
          0.9989
        
        
          4
        
        
          Fenpropathrin
        
        
          0-200
        
        
          0.9981
        
        
          7
        
        
          0.9972
        
        
          45
        
        
          0.9146
        
        
          6
        
        
          Fenpropidin
        
        
          0-1000
        
        
          0.9998
        
        
          18
        
        
          0.9997
        
        
          7
        
        
          0.9962
        
        
          17
        
        
          Fenpropimorph
        
        
          0-200
        
        
          0.9998
        
        
          10
        
        
          0.9997
        
        
          5
        
        
          0.9943
        
        
          27
        
        
          Fenthion
        
        
          0-200
        
        
          0.9987
        
        
          17
        
        
          0.9998
        
        
          21
        
        
          0.9997
        
        
          5
        
        
          Fenvalerate
        
        
          0-200
        
        
          0.9999
        
        
          10
        
        
          0.9949
        
        
          84
        
        
          0.9973
        
        
          19
        
        
          Fipronil
        
        
          0-200
        
        
          0.9998
        
        
          8
        
        
          0.9984
        
        
          26
        
        
          0.9991
        
        
          29
        
        
          Fludioxonil
        
        
          0-200
        
        
          0.9800
        
        
          1
        
        
          0.9979
        
        
          11
        
        
          0.9992
        
        
          23
        
        
          Fluquinconazole
        
        
          0-200
        
        
          0.9976
        
        
          22
        
        
          0.9990
        
        
          153
        
        
          0.9995
        
        
          39
        
        
          Flusilazole
        
        
          0-200
        
        
          0.9984
        
        
          2
        
        
          0.9953
        
        
          13
        
        
          0.9977
        
        
          11
        
        
          Flutolanil
        
        
          0-200
        
        
          0.9989
        
        
          15
        
        
          0.9996
        
        
          38
        
        
          0.9997
        
        
          7
        
        
          Flutriafol
        
        
          0-200
        
        
          0.9996
        
        
          1
        
        
          0.9991
        
        
          14
        
        
          0.9996
        
        
          23
        
        
          Fluvalinate
        
        
          0-200
        
        
          0.9995
        
        
          20
        
        
          0.9956
        
        
          131
        
        
          0.9938
        
        
          1
        
        
          Folpet
        
        
          0-2000 0.9959
        
        
          76
        
        
          0.9984
        
        
          48
        
        
          n.d.
        
        
          n.d.
        
        
          n.d.
        
        
          HCH alpha
        
        
          0-200
        
        
          0.9999
        
        
          8
        
        
          0.9951
        
        
          8
        
        
          0.9977
        
        
          15
        
        
          HCH beta
        
        
          0-200
        
        
          0.9999
        
        
          14
        
        
          0.9993
        
        
          16
        
        
          0.9981
        
        
          29
        
        
          HCH gamma_Lindane
        
        
          0-200
        
        
          0.9999
        
        
          12
        
        
          0.9945
        
        
          17
        
        
          0.9961
        
        
          21
        
        
          Hexaconazole
        
        
          0-1000
        
        
          0.9938
        
        
          8
        
        
          0.9995
        
        
          11
        
        
          0.9999
        
        
          11
        
        
          Imazalil
        
        
          0-1000
        
        
          0.9987
        
        
          14
        
        
          0.9985
        
        
          14
        
        
          0.9998
        
        
          26
        
        
          Iprodione
        
        
          0-200
        
        
          0.9981
        
        
          5
        
        
          0.9984
        
        
          34
        
        
          0.9917
        
        
          13
        
        
          Isofenphos-methyl
        
        
          0-200
        
        
          0.9996
        
        
          6
        
        
          0.9996
        
        
          54
        
        
          0.9992
        
        
          6
        
        
          Kresoxim-methyl
        
        
          0-200
        
        
          0.9990
        
        
          15
        
        
          0.9974
        
        
          15
        
        
          0.9992
        
        
          35
        
        
          Linuron
        
        
          0-1000
        
        
          0.9986
        
        
          50
        
        
          0.9967
        
        
          55
        
        
          0.9996
        
        
          42
        
        
          Malathion
        
        
          0-200
        
        
          0.9985
        
        
          14
        
        
          0.9995
        
        
          11
        
        
          0.9816
        
        
          30
        
        
          Mepanipyrim
        
        
          0-200
        
        
          0.9993
        
        
          24
        
        
          0.9928
        
        
          38
        
        
          0.9995
        
        
          11
        
        
          Metalaxyl
        
        
          0-1000
        
        
          0.9999
        
        
          20
        
        
          0.9996
        
        
          30
        
        
          0.9980
        
        
          37
        
        
          Methacrifos
        
        
          0-200
        
        
          0.9994
        
        
          3
        
        
          0.9983
        
        
          16
        
        
          0.9951
        
        
          19
        
        
          13
        
        
          
            Compound
          
        
        
          
            Calibration
          
        
        
          
            Range
          
        
        
          
            [ng/g]
          
        
        
          
            Strawberry
          
        
        
          
            Wheat Flour
          
        
        
          
            Leek
          
        
        
          
            r2
          
        
        
          
            Residue
          
        
        
          
            Plot
          
        
        
          
            Deviation
          
        
        
          
            [%RSD]
          
        
        
          
            Youden
          
        
        
          
            Plot
          
        
        
          
            Slope
          
        
        
          
            [diff%]
          
        
        
          
            r2
          
        
        
          
            Residue
          
        
        
          
            Plot
          
        
        
          
            Deviation
          
        
        
          
            [%RSD]
          
        
        
          
            Youden
          
        
        
          
            Plot
          
        
        
          
            Slope
          
        
        
          
            [diff%]
          
        
        
          
            r2
          
        
        
          
            Residue
          
        
        
          
            Plot
          
        
        
          
            Deviation
          
        
        
          
            [%RSD]
          
        
        
          
            Youden
          
        
        
          
            Plot
          
        
        
          
            Slope
          
        
        
          
            [diff%]
          
        
        
          
            Table 3 continued
          
        
        
          – residue plot RSD% <20%
        
        
          – residue plot RSD% >20%
        
        
       
      
        
          1...,67,68,69,70,71,72,73,74,75,76
        
        
          78,79,80,81,82,83,84,85,86,87,...225