Fenpropimorph
7
11
3
7
14
6
8
8
18
10
9
9
Fenthion
16
5
6
13
30
12
9
48
12
13
5
10
Fenvalerate
5
8
3
7
7
2
3
2
3
4
12
9
Fipronil
8
5
3
7
24
4
18
17
11
4
4
17
Fludioxonil
<LOD <LOD 6
n.d.
7
5 46
5
6
9
5
8
Fluquinconazole
7
7
5
7
13
4
4
11
3
6
10
16
Flusilazole
12
14
3
9
7
7
4
7
14
15
6
15
Flutolanil
5
2
2
5
8
4
6
5
4
8
8
8
Flutriafol
6
1
2
5
23
2 40
5
6
6
7
8
Fluvalinate
8
12
5
9
6
5
4
4
9
14
14
14
Folpet**
30
71 21
74
27
12 43
22
<LOD <LOD <LOQ
n.d.
HCH alpha
7
9
3
6
9
4
11
5
3
8
5
13
HCH beta
7
8
3
7
18
4
10
7
7
8
7
12
HCH gamma_Lindane
10
9
1
7
12
4
11
4
10
9
6
10
Hexaconazole*
14
12
3
9
11
6
4
7
13
4
10
8
Imazalil*
7
4
3
4
9
5
10
4
6
4
10
8
Iprodione
12
4
4
5
6
5
8
7
7
7
11
10
Isofenphos-methyl
3
3
3
3
13
4
9
6
4
4
7
7
Kresoxim-methyl
1
6
4
5
5
2
5
3
8
4
6
5
Linuron*
5
5
7
18
18
6 20
12
5
4
10
9
Malathion
3
8
4
8
14
4
14
10
10
11
10
12
Mepanipyrim
10
4
3
6
13
4 22
8
4
7
9
5
Metalaxyl*
5
5
5
5
17
5
12
6
2
7
4
6
Methacrifos
11
11
3
7
75
3
17
8
7
11
6
11
Methamidophos
15
12
14
31
23
7 25
8
7
14
9
22
Methidathion
6
7
5
7
14
3
13
5
5
4
8
6
Methiocarb**
15
15
5
17
<LOD <LOD 11*
n.d.
<LOD <LOQ 11
n.d.
Metribuzin*
8
7
6
9
15
5
11
6
5
7
7
7
Monocrotophos*
13
13
11
20
9
2
13
6
6
15
10
18
Myclobutanil
5
3
3
6
1
5
3
4
6
9
5
7
Ortho-phenylphenol
4
7
3
6
31
12
15
20
4
8
6
6
Oxadiazon
3
9
4
7
5
4
6
4
9
8
6
8
Oxadixyl
4
4
4
5
8
2
4
3
7
5
8
8
Paclobutrazol
3
6
5
4
16
4
10
7
4
4
8
6
Paraoxon-methyl*
7
10
12
17
12
4
17
10
4
16
16
16
Parathion (ethyl)*
8
10
3
12
25
8
11
17
4
5
7
5
Parathion-methyl
13
11
6
9
8
7
12
8
4
5
7
4
Pendimethalin
22
20
5
25
17
13
11
32
8
9
6
14
Permethrin
3
4
3
4
2
3
4
3
4
10
11
8
Phenthoate*
5
7
4
6
5
3
13
23
3
5
8
4
Phosalone
2
5
2
4
42
3
3
22
4
10
8
10
Phosmet
7
10
9
14
6
1
8
4
6 23
13
26
Phosphamidon
7
9
10
21
20
2
15
8
76 42 24
62
Compound
Strawberry
Wheat Flour
Leek
Precision
Intermediate
Precision
Precision
Intermediate
Precision
Precision
Intermediate
Precision
Level
1
Level
2
Level
3
Level
1
Level
2
Level
3
Level
1
Level
2
Level
3
Table 5 continued
* spiking levels are 50, 100 & 500 ** spiking levels are 100, 200 & 1000 <LOD/LOQ – spiking value below LOD/LOQ value
20
