 
          Pirimicarb
        
        
          9
        
        
          7
        
        
          5
        
        
          6
        
        
          13
        
        
          5
        
        
          12
        
        
          6
        
        
          7
        
        
          9
        
        
          6
        
        
          7
        
        
          Pirimicarb-p-desmetyl*
        
        
          12
        
        
          16
        
        
          8
        
        
          11
        
        
          13
        
        
          3
        
        
          12
        
        
          5
        
        
          4
        
        
          8
        
        
          9
        
        
          5
        
        
          Pirimiphos methyl
        
        
          6
        
        
          6
        
        
          4
        
        
          5
        
        
          10
        
        
          4
        
        
          11
        
        
          22
        
        
          6
        
        
          7
        
        
          6
        
        
          5
        
        
          Prochloraz*
        
        
          4
        
        
          3
        
        
          4
        
        
          7
        
        
          9
        
        
          5
        
        
          7
        
        
          10
        
        
          5
        
        
          6
        
        
          14
        
        
          6
        
        
          Procymidone
        
        
          8
        
        
          6
        
        
          4
        
        
          7
        
        
          16
        
        
          2
        
        
          8
        
        
          10
        
        
          8
        
        
          6
        
        
          7
        
        
          9
        
        
          Profenofos
        
        
          19
        
        
          12
        
        
          7
        
        
          13
        
        
          14
        
        
          8
        
        
          12
        
        
          12
        
        
          13 27
        
        
          12
        
        
          31
        
        
          Propargite
        
        
          5
        
        
          4
        
        
          4
        
        
          11
        
        
          <LOD <LOD 56
        
        
          n.d.
        
        
          10
        
        
          9
        
        
          8
        
        
          16
        
        
          Propiconazole
        
        
          2
        
        
          2
        
        
          3
        
        
          4
        
        
          8
        
        
          4
        
        
          11
        
        
          3
        
        
          3
        
        
          6
        
        
          8
        
        
          6
        
        
          Propyzamide
        
        
          4
        
        
          6
        
        
          3
        
        
          5
        
        
          11
        
        
          3
        
        
          11
        
        
          5
        
        
          2
        
        
          7
        
        
          5
        
        
          5
        
        
          Prothiofos
        
        
          9
        
        
          3
        
        
          4
        
        
          6
        
        
          17
        
        
          5
        
        
          8
        
        
          17
        
        
          8
        
        
          10
        
        
          6
        
        
          11
        
        
          Pyraclostrobin
        
        
          5
        
        
          3
        
        
          3
        
        
          8
        
        
          2
        
        
          2
        
        
          3
        
        
          2
        
        
          2
        
        
          3
        
        
          11
        
        
          5
        
        
          Pyridaben
        
        
          3
        
        
          2
        
        
          3
        
        
          4
        
        
          3
        
        
          2
        
        
          2
        
        
          3
        
        
          6
        
        
          8
        
        
          12
        
        
          9
        
        
          Pyrimethanil
        
        
          4
        
        
          7
        
        
          2
        
        
          6
        
        
          13
        
        
          3
        
        
          8
        
        
          5
        
        
          3
        
        
          9
        
        
          7
        
        
          6
        
        
          Pyriproxyfen
        
        
          3
        
        
          4
        
        
          2
        
        
          4
        
        
          4
        
        
          1
        
        
          3
        
        
          1
        
        
          2
        
        
          4
        
        
          8
        
        
          6
        
        
          Quinoxyfen
        
        
          2
        
        
          4
        
        
          2
        
        
          3
        
        
          4
        
        
          2
        
        
          2
        
        
          5
        
        
          5
        
        
          3
        
        
          8
        
        
          3
        
        
          Spirodiclofen
        
        
          10
        
        
          6
        
        
          5
        
        
          13
        
        
          14
        
        
          5
        
        
          10
        
        
          10
        
        
          <LOQ 11
        
        
          12
        
        
          17
        
        
          Tebuconazole
        
        
          3
        
        
          2
        
        
          1
        
        
          3
        
        
          6
        
        
          3
        
        
          7
        
        
          2
        
        
          3
        
        
          3
        
        
          9
        
        
          7
        
        
          Tebufenocide*
        
        
          6
        
        
          5
        
        
          2
        
        
          6
        
        
          <LOD <LOQ 6
        
        
          7
        
        
          <LOQ 6
        
        
          9
        
        
          7
        
        
          Tebufenpyrad
        
        
          3
        
        
          6
        
        
          3
        
        
          5
        
        
          18
        
        
          7
        
        
          10
        
        
          16
        
        
          3
        
        
          8
        
        
          8
        
        
          6
        
        
          Tefluthrin
        
        
          7
        
        
          7
        
        
          4
        
        
          5
        
        
          16
        
        
          5
        
        
          11
        
        
          6
        
        
          4
        
        
          8
        
        
          6
        
        
          6
        
        
          Tetraconazole*
        
        
          4
        
        
          6
        
        
          4
        
        
          4
        
        
          13
        
        
          4
        
        
          11
        
        
          6
        
        
          4
        
        
          4
        
        
          6
        
        
          4
        
        
          Tetradifon
        
        
          11
        
        
          7
        
        
          4
        
        
          5
        
        
          7
        
        
          2
        
        
          6
        
        
          4
        
        
          7
        
        
          6
        
        
          7
        
        
          7
        
        
          Tetrahydrophthalimide (THPI) <LOQ <LOQ 8
        
        
          n.d.
        
        
          <LOQ 27
        
        
          11
        
        
          23
        
        
          <LOQ 9
        
        
          6
        
        
          8
        
        
          Thiabendazole*
        
        
          5
        
        
          3
        
        
          4
        
        
          3
        
        
          16
        
        
          3
        
        
          14
        
        
          6
        
        
          4
        
        
          5
        
        
          9
        
        
          7
        
        
          Tolclofos-methyl
        
        
          4
        
        
          6
        
        
          6
        
        
          9
        
        
          15
        
        
          6
        
        
          15
        
        
          18
        
        
          5
        
        
          8
        
        
          5
        
        
          20
        
        
          Tolyfluanid*
        
        
          9
        
        
          22
        
        
          10
        
        
          20
        
        
          21
        
        
          8
        
        
          17
        
        
          10
        
        
          n.d.
        
        
          n.d.
        
        
          n.d.
        
        
          n.d.
        
        
          Triadimefon*
        
        
          4
        
        
          4
        
        
          2
        
        
          5
        
        
          12
        
        
          3
        
        
          9
        
        
          6
        
        
          1
        
        
          6
        
        
          6
        
        
          7
        
        
          Triadimenol*
        
        
          9
        
        
          7
        
        
          3
        
        
          7
        
        
          10
        
        
          3
        
        
          9
        
        
          10
        
        
          9
        
        
          7
        
        
          7
        
        
          5
        
        
          Trifloxystrobin
        
        
          4
        
        
          4
        
        
          2
        
        
          3
        
        
          6
        
        
          4
        
        
          3
        
        
          3
        
        
          4
        
        
          8
        
        
          8
        
        
          6
        
        
          Trifluralin
        
        
          3
        
        
          16
        
        
          8
        
        
          17
        
        
          1
        
        
          12
        
        
          13
        
        
          20
        
        
          2
        
        
          12
        
        
          8
        
        
          32
        
        
          Triticonazole
        
        
          7
        
        
          3
        
        
          3
        
        
          3
        
        
          4
        
        
          3
        
        
          2
        
        
          3
        
        
          5
        
        
          6
        
        
          9
        
        
          6
        
        
          Vinclozolin
        
        
          15
        
        
          4
        
        
          6
        
        
          8
        
        
          16
        
        
          6
        
        
          14
        
        
          14
        
        
          23
        
        
          9
        
        
          7
        
        
          10
        
        
          
            Compound
          
        
        
          
            Strawberry
          
        
        
          
            Wheat Flour
          
        
        
          
            Leek
          
        
        
          
            Precision
          
        
        
          
            Intermediate
          
        
        
          
            Precision
          
        
        
          
            Precision
          
        
        
          
            Intermediate
          
        
        
          
            Precision
          
        
        
          
            Precision
          
        
        
          
            Intermediate
          
        
        
          
            Precision
          
        
        
          
            Level
          
        
        
          
            1
          
        
        
          
            Level
          
        
        
          
            2
          
        
        
          
            Level
          
        
        
          
            3
          
        
        
          
            Level
          
        
        
          
            1
          
        
        
          
            Level
          
        
        
          
            2
          
        
        
          
            Level
          
        
        
          
            3
          
        
        
          
            Level
          
        
        
          
            1
          
        
        
          
            Level
          
        
        
          
            2
          
        
        
          
            Level
          
        
        
          
            3
          
        
        
          
            Table 5 continued
          
        
        
          * spiking levels are 50, 100 & 500    ** spiking levels are 100, 200 & 1000    <LOD/LOQ – spiking value below LOD/LOQ value
        
        
          21