HCH alpha
79
109
87
113
121
88
84
135
108
HCH beta
85
111
90
109
110
85
87
138
109
HCH gamma_Lindane
87
110
89
115
123
88
81
132
106
Hexaconazole*
95
97
84
95
103
75
90
111
88
Imazalil*
72
97
84
87
102
67
69
96
78
Iprodione
109
111
86
120
124
94
109
102
84
Isofenphos-methyl
85
111
92
99
112
89
94
128
103
Kresoxim-methyl
86
111
96
114
119
85
86
120
101
Linuron*
126
118
95
95
100
63
126
133
98
Malathion
108
106
90
83
122
101
150
121
88
Mepanipyrim
82
111
96
123
138
72
93
121
95
Metalaxyl*
84
111
91
97
115
90
75
115
95
Methacrifos
89
108
78
82
109
96
66
130
103
Methamidophos
56
60
63
59
61
50
97
73
51
Methidathion
110
106
84
99
118
94
106
125
98
Methiocarb**
85
98
81
<LOD
<LOD
75
<LOD
<LOQ
78
Metribuzin*
87
111
98
89
117
84
94
129
99
Monocrotophos*
90
92
74
110
99
60
107
87
63
Myclobutanil
91
115
96
104
109
83
77
116
94
Ortho-phenylphenol
95
102
74
63
75
78
61
120
99
Oxadiazon
84
115
95
111
117
81
69
117
100
Oxadixyl
89
108
87
116
118
84
76
108
93
Paclobutrazol
81
106
91
95
109
85
90
111
91
Paraoxon-methyl*
102
108
109
137
146
111
132
117
73
Parathion (ethyl)*
69
98
101
54
95
95
120
132
100
Parathion-methyl
83
107
98
108
129
95
101
138
105
Pendimethalin
45
81
118
51
73
85
117
132
96
Permethrin
109
107
83
109
115
81
91
112
94
Phenthoate*
83
111
105
124
124
95
99
125
97
Phosalone
115
106
82
97
87
83
103
108
86
Phosmet
114
87
71
104
115
88
107
85
63
Phosphamidon
109
112
95
115
131
98
53
64
120
Pirimicarb
85
110
87
90
113
90
77
118
94
Pirimicarb-p-desmetyl*
79
99
81
85
106
82
82
122
89
Pirimiphos methyl
90
109
93
116
113
93
71
111
92
Prochloraz*
117
94
72
112
124
87
76
86
71
Procymidone
85
107
87
84
115
86
82
119
98
Profenofos
112
107
89
112
108
90
119
89
77
Propargite
104
104
90
<LOD
<LOD
58
62
89
88
Propiconazole
89
95
74
102
110
77
79
107
90
Propyzamide
84
110
89
100
116
88
90
133
103
Prothiofos
73
96
92
95
99
82
89
104
81
Pyraclostrobin
100
116
90
128
139
97
101
123
92
Pyridaben
111
110
86
108
114
81
92
108
87
Pyrimethanil
78
103
84
84
103
84
70
118
95
17
Table 4 continued
* spiking levels are 50, 100 & 500 ng/g ** spiking levels are 100, 200 & 1000 ng/g <LOD/LOQ – spiking value below LOD/LOQ value
Compound
Strawberry
Wheat Flour
Leek
Level 1
Level 2
Level 3
Level 1
Level 2
Level 3
Level 1
Level 2
Level 3
