 
       
     
    
      AI10382-GC-MS-Food Safety-Analysis - page 78
      
              
          Methamidophos
        
        
          0-200
        
        
          0.9995
        
        
          0
        
        
          0.9995
        
        
          9
        
        
          0.9967
        
        
          33
        
        
          Methidathion
        
        
          0-200
        
        
          0.9984
        
        
          13
        
        
          0.9997
        
        
          14
        
        
          0.9988
        
        
          32
        
        
          Methiocarb
        
        
          0-2000 0.9988
        
        
          2
        
        
          0.9963
        
        
          20
        
        
          0.9876
        
        
          33
        
        
          Metribuzin
        
        
          0-1000
        
        
          0.9997
        
        
          21
        
        
          0.9996
        
        
          22
        
        
          0.9995
        
        
          28
        
        
          Monocrotophos
        
        
          0-1000
        
        
          0.9997
        
        
          36
        
        
          0.9990
        
        
          11
        
        
          0.9982
        
        
          45
        
        
          Myclobutanil
        
        
          0-200
        
        
          0.9994
        
        
          2
        
        
          0.9979
        
        
          8
        
        
          0.9991
        
        
          20
        
        
          Ortho-phenylphenol
        
        
          0-200
        
        
          0.9999
        
        
          4
        
        
          0.9995
        
        
          18
        
        
          0.9945
        
        
          24
        
        
          Oxadiazon
        
        
          0-200
        
        
          0.9999
        
        
          8
        
        
          0.9968
        
        
          11
        
        
          0.9956
        
        
          28
        
        
          Oxadixyl
        
        
          0-200
        
        
          0.9997
        
        
          5
        
        
          0.9969
        
        
          4
        
        
          0.9989
        
        
          25
        
        
          Paclobutrazol
        
        
          0-200
        
        
          0.9996
        
        
          4
        
        
          0.9997
        
        
          1
        
        
          0.9988
        
        
          15
        
        
          Paraoxon-methyl
        
        
          0-1000
        
        
          0.9957
        
        
          40
        
        
          0.9964
        
        
          27
        
        
          0.9875
        
        
          43
        
        
          Parathion (ethyl)
        
        
          0-1000
        
        
          0.9968
        
        
          7
        
        
          0.9956
        
        
          4
        
        
          0.9964
        
        
          20
        
        
          Parathion-methyl
        
        
          0-200
        
        
          0.9996
        
        
          24
        
        
          0.9985
        
        
          30
        
        
          0.9997
        
        
          35
        
        
          Pendimethalin
        
        
          0-200
        
        
          0.9950
        
        
          15
        
        
          0.9910
        
        
          121
        
        
          0.9937
        
        
          75
        
        
          Permethrin
        
        
          0-200
        
        
          0.9951
        
        
          27
        
        
          0.9961
        
        
          70
        
        
          0.9970
        
        
          13
        
        
          Phenthoate
        
        
          0-1000
        
        
          0.9991
        
        
          18
        
        
          0.9989
        
        
          25
        
        
          0.9996
        
        
          32
        
        
          Phosalone
        
        
          0-200
        
        
          0.9976
        
        
          2
        
        
          0.9921
        
        
          33
        
        
          0.9939
        
        
          12
        
        
          Phosmet
        
        
          0-200
        
        
          0.9972
        
        
          28
        
        
          0.9961
        
        
          34
        
        
          0.9922
        
        
          61
        
        
          Phosphamidon
        
        
          0-200
        
        
          0.9989
        
        
          42
        
        
          0.9997
        
        
          37
        
        
          0.9961
        
        
          70
        
        
          Pirimicarb
        
        
          0-200
        
        
          0.9998
        
        
          16
        
        
          0.9997
        
        
          22
        
        
          0.9990
        
        
          32
        
        
          Pirimicarb-p-desmetyl
        
        
          0-1000
        
        
          0.9999
        
        
          26
        
        
          0.9998
        
        
          28
        
        
          0.9994
        
        
          36
        
        
          Pirimiphos methyl
        
        
          0-200
        
        
          0.9987
        
        
          15
        
        
          0.9980
        
        
          4
        
        
          0.9986
        
        
          25
        
        
          Prochloraz
        
        
          0-1000
        
        
          0.9924
        
        
          9
        
        
          0.9974
        
        
          37
        
        
          0.9925
        
        
          12
        
        
          Procymidone
        
        
          0-200
        
        
          0.9999
        
        
          17
        
        
          0.9996
        
        
          6
        
        
          0.9969
        
        
          26
        
        
          Profenofos
        
        
          0-200
        
        
          0.9988
        
        
          2
        
        
          0.9992
        
        
          >200
        
        
          0.9940
        
        
          34
        
        
          Propargite
        
        
          0-200
        
        
          0.9991
        
        
          9
        
        
          0.8967
        
        
          17
        
        
          0.9997
        
        
          51
        
        
          Propiconazole
        
        
          0-200
        
        
          0.9986
        
        
          13
        
        
          0.9976
        
        
          15
        
        
          0.9877
        
        
          10
        
        
          Propyzamide
        
        
          0-200
        
        
          0.9999
        
        
          9
        
        
          0.9995
        
        
          14
        
        
          0.9946
        
        
          25
        
        
          Prothiofos
        
        
          0-200
        
        
          0.9993
        
        
          20
        
        
          0.9987
        
        
          80
        
        
          0.9986
        
        
          4
        
        
          Pyraclostrobin
        
        
          0-200
        
        
          0.9997
        
        
          6
        
        
          0.9954
        
        
          56
        
        
          0.9964
        
        
          1
        
        
          Pyridaben
        
        
          0-200
        
        
          0.9961
        
        
          29
        
        
          0.9967
        
        
          79
        
        
          0.9953
        
        
          14
        
        
          Pyrimethanil
        
        
          0-200
        
        
          0.9999
        
        
          13
        
        
          0.9997
        
        
          13
        
        
          0.9963
        
        
          20
        
        
          Pyriproxyfen
        
        
          0-200
        
        
          0.9982
        
        
          1
        
        
          0.9964
        
        
          12
        
        
          0.9996
        
        
          17
        
        
          Quinoxyfen
        
        
          0-200
        
        
          0.9977
        
        
          15
        
        
          0.9979
        
        
          28
        
        
          0.9998
        
        
          2
        
        
          Spirodiclofen
        
        
          0-200
        
        
          0.9995
        
        
          7
        
        
          0.9974
        
        
          8
        
        
          0.9950
        
        
          34
        
        
          Tebuconazole
        
        
          0-200
        
        
          0.9995
        
        
          17
        
        
          0.9969
        
        
          22
        
        
          0.9986
        
        
          3
        
        
          Tebufenocide
        
        
          0-1000
        
        
          0.9980
        
        
          11
        
        
          0.9975
        
        
          34
        
        
          0.9984
        
        
          12
        
        
          Tebufenpyrad
        
        
          0-200
        
        
          0.9987
        
        
          8
        
        
          0.9996
        
        
          126
        
        
          0.9996
        
        
          4
        
        
          Tefluthrin
        
        
          0-200
        
        
          1.0000
        
        
          14
        
        
          0.9994
        
        
          20
        
        
          0.9929
        
        
          31
        
        
          Tetraconazole
        
        
          0-1000
        
        
          0.9997
        
        
          17
        
        
          0.9997
        
        
          13
        
        
          0.9975
        
        
          33
        
        
          Tetradifon
        
        
          0-200
        
        
          0.9998
        
        
          10
        
        
          0.9959
        
        
          11
        
        
          0.9989
        
        
          30
        
        
          Tetrahydrophthalimide
        
        
          0-200
        
        
          0.9645
        
        
          106
        
        
          0.9638
        
        
          51
        
        
          0.8388
        
        
          93
        
        
          14
        
        
          
            Compound
          
        
        
          
            Calibration
          
        
        
          
            Range
          
        
        
          
            [ng/g]
          
        
        
          
            Strawberry
          
        
        
          
            Wheat Flour
          
        
        
          
            Leek
          
        
        
          
            r2
          
        
        
          
            Residue
          
        
        
          
            Plot
          
        
        
          
            Deviation
          
        
        
          
            [%RSD]
          
        
        
          
            Youden
          
        
        
          
            Plot
          
        
        
          
            Slope
          
        
        
          
            [diff%]
          
        
        
          
            r2
          
        
        
          
            Residue
          
        
        
          
            Plot
          
        
        
          
            Deviation
          
        
        
          
            [%RSD]
          
        
        
          
            Youden
          
        
        
          
            Plot
          
        
        
          
            Slope
          
        
        
          
            [diff%]
          
        
        
          
            r2
          
        
        
          
            Residue
          
        
        
          
            Plot
          
        
        
          
            Deviation
          
        
        
          
            [%RSD]
          
        
        
          
            Youden
          
        
        
          
            Plot
          
        
        
          
            Slope
          
        
        
          
            [diff%]
          
        
        
          
            Table 3 continued
          
        
        
          – residue plot RSD% <20%
        
        
          – residue plot RSD% >20%
        
        
       
      
        
          1...,68,69,70,71,72,73,74,75,76,77
        
        
          79,80,81,82,83,84,85,86,87,88,...225