2
Reagents
Part Number
Thermo Scientific MBTFA 10 x 1 mL ampules
TS-49700
Thermo Scientific pyridine silylation grade solvent
TS-27530
Sample Handling Equipment
Part Number
Thermo Scientific Reacti-Therm III Heating/Stirring Module
TS-18823
Thermo Scientific Reacti-Vap III Evaporator
TS-18826
Thermo Scientific Reacti-Block Q-1 (Holds 8 x 10 mL Reacti-Vials)
TS-18814
Thermo Scientific Reacti-Vial clear glass reaction vials 10 mL
TS-13225
Thermo Scientific 2 mL amber vial and screw tops
60180-565
Separation Conditions
Part Number
Instrumentation:
Thermo Scientific TRACE GC Ultra
Column:
TRACE™ TR-1701
260Q142P
30 m × 0.25 mm × 0.25 μm
Thermo Scientific BTO 17 mm septa
31303211
5 mm ID focus split liner, 105 mm long
453T1905
Graphite liner seal
29033406
10 μL, 50 mm needle length gauge 25 Syringe
36500525
Graphite ferrules to fit 0.1-0.25 mm ID columns
29053488
Carrier gas:
Helium
Split flow:
60 mL/min
Column flow:
1.2 mL/min, Constant flow
Split ratio:
1:1
Oven temperature:
40 °C (1 min), 10 °C/min, 260 °C (5 min)
Injector type:
Split/Splitless
Injector mode:
Split
Injector temperature:
200 °C
Detector type:
FID
Detector temperature:
250 °C
Detector air flow:
35 mL/min
Detector Hydrogen flow:
350 mL/min
Detector nitrogen flow:
30 mL/min
Thermo Scientific TriPlus Autosampler
Injection Volume:
1 μL
Data Processing
Software:
Thermo Scientific XCalibur
