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4

Calibration Curves

Calibration curves were produced in the range of 2 µg/L

to 700 µg/L for the OCPs and PCBs. A higher range,

2 µg/L to 2,500 µg/L, was necessary for the PAHs. The

curves were not corrected for internal standard calibration.

All curves had a regression coefficient higher than 0.995.

Curves for a selection of target compounds are plotted in

Figures 3 & 4.

a: naphthalene with R

2

=0.9991

b: phenanthrene with R

2

= 0.9994

c: benzo(a) anthracene with R

2

= 0.9985

d: fluorene with R

2

= 0.9998

e: benzoperylene with R

2

= 0.9993

a: PCB153 with R

2

=0.9999

b: aldrin with R

2

= 0.9993

c: alpha endosulfan with R

2

= 0.9996

d: tetrachlorobenzene with R

2

= 0.9999

e: trifluralin with R

2

= 0.9999

a

d

b

e

c

a

d

b

e

c

Figure 3: Calibration curves of various PAHs. The compounds and their respective regression coefficients were:

Figure 4: Calibration curves of various pesticides. The compounds and their respective regression coefficients were: