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9

Parent Mass

(Da)

Product Mass

(Da)

Collision Energy

(V)

RT

(min)

Start Time

*

(min)

Stop Time

*

(min)

Name

218.89

182.91

8

7.14

6.64

7.64 BHC-delta Confirming 1

216.89

180.91

8

7.24

6.74

7.74 BHC-epsilon

218.89

182.91

8

7.24

6.74

7.74 BHC-epsilon Confirming 1

188.14

160.00

30

7.53

7.03

8.03 Alachlor Confirming 1

188.14

158.00

30

7.53

7.03

8.03 Alachlor

352.83

252.88

15

8.60

8.10

9.10 Heptachlor exo-epoxide (isomer B)

352.83

281.88

15

8.60

8.10

9.10 Heptachlor exo-epoxide (isomer B) Confirming 1

288.86

252.88

15

8.65

8.15

9.15 Heptachlor endo-epoxide (isomer A) Confirming 1

288.86

218.95

15

8.65

8.15

9.15 Heptachlor endo-epoxide (isomer A)

246.05

175.97

25

8.93

8.43

9.43 DDE-o,p'

317.94

245.95

20

8.93

8.43

9.43 DDE-o,p' Confirming 1

325.88

255.91

20

8.99

8.49

9.49 2,2',4,5,5'-Pentachlorobiphenyl (BZ #101) Confirming 1

323.88

253.91

20

8.99

8.49

9.49 2,2',4,5,5'-Pentachlorobiphenyl (BZ #101)

202.08

200.08

30

9.10

8.60

9.60 pyrene Confirming 1

202.08

176.08

35

9.10

8.60

9.60 pyrene

246.05

175.97

25

9.39

8.89

9.89 DDE-p,p'

317.94

245.95

20

9.39

8.89

9.89 DDE-p,p' Confirming 1

242.89

207.91

10

9.95

9.45

10.45 Endosulfan II (beta isomer) Confirming 1

240.89

205.91

10

9.95

9.45

10.45 Endosulfan II (beta isomer)

235.01

164.98

20

10.00

9.52

10.52 DDD-p,p'

237.01

164.98

20

10.00

9.52

10.52 DDD-p,p' Confirming 1

237.01

165.07

20

10.10

9.56

10.56 DDT-o,p' Confirming 1

235.01

165.07

20

10.10

9.56

10.56 DDT-o,p'

359.84

289.87

25

10.60

10.13

11.13

2,2',3,4,4',5'-Hexachlorobiphenyl (BZ #138)

Confirming 1

357.84

287.88

25

10.60

10.13

11.13 2,2',3,4,4',5'-Hexachlorobiphenyl (BZ #138)

237.01

165.07

20

10.50

10.03

11.03 DDT-p,p' Confirming 1

235.01

165.07

20

10.50

10.03

11.03 DDT-p,p'

228.08

202.08

35

11.50

11.00

12.00 benzo[a]anthracene

228.08

226.08

30

11.50

11.00

12.00 benzo[a]anthracene Confirming 1

228.08

202.08

35

11.40

10.94

11.94 chrysene

228.08

226.08

30

11.40

10.94

11.94 chrysene Confirming 1

252.09

226.08

35

13.60

13.12

14.12 benzo[b]fluoranthene

252.09

250.09

30

13.60

13.12

14.12 benzo[b]fluoranthene Confirming 1

252.09

250.09

30

14.30

13.76

14.76 benzo[a]pyrene Confirming 1

252.09

226.08

35

14.30

13.76

14.76 benzo[a]pyrene

252.09

250.09

30

13.70

13.21

14.21 benzo[k]fluoranthene Confirming 1

252.09

226.08

35

13.70

13.21

14.21 benzo[k]fluoranthene

202.08

176.08

35

8.72

8.22

9.22 fluoranthene Confirming 1

202.08

200.08

30

8.72

8.22

9.22 fluoranthene

292.90

185.93

30

8.11

7.61

8.61 Aldrin

292.90

257.91

10

8.11

7.61

8.61 Aldrin Confirming 1

262.91

192.93

30

8.48

7.98

8.98 Isodrin

262.91

190.93

30

8.48

7.98

8.98 Isodrin Confirming 1

240.89

205.91

10

9.11

8.61

9.61 Endosulfan I (alpha isomer)

242.89

207.91

10

9.11

8.61

9.61 Endosulfan I (alpha isomer) Confirming 1

*

Start and Stop Times are set automatically in timed-SRM mode of the TSQ 8000 by using a standard acquisition window of 60 s for all compounds