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High Density Sample Report 1 Long
Lab Name:
Clinical Marketing
Page 1 of 1
Instrument:
TSQ Quantum Ultra
Method: 20110707_Opiods3
User:
Thermo Scientific
Batch:
20110707
Cali File: 20110707.calx
Vial Pos
Sample ID
File Name
Level
Sample Name
File Date
Comment
CStk1-03:2
20ng
20ng
7/8/2011 4:23:59 PM processed 22Jun2011
Meperidine
Quan
m/z
: 220.11
Total Area: 246644
Peak Area: 246644
RT: 1.57 min (1.56)
TAmount: 20.000 ng/mL
Amount: 22.452 ng/mL
Normeperidine
Quan
m/z
: 160.12
Total Area: 11446
Peak Area: 11446
RT: 1.72min (1.70)
TAmount: 2.000 ng/mL
Amount: 1.844 ng/mL
Normeperidine-d4
Quan
m/z
: 164.20
Total Area: 2478539
Peak Area: 2478539
RT: 1.71min (1.70)
Amount: 1.000
EDDP-d3
Quan
m/z
: 234.10
Total Area: 5101141
Peak Area: 5101141
RT: 2.34 min (2.34)
Amount: 1.000
Norpropoxyphene-d5
Quan
m/z
: 100.10
Total Area: 412479
Peak Area: 412479
RT: 2.64min (2.63)
Amount: 1.000
Norpropoxyphene
Quan
m/z
: 100.10
Total Area: 31463
Peak Area: 31463
RT: 2.64 min (2.64)
TAmount: 20.000 ng/mL
Amount: 22.669 ng/mL
Propoxyphene
Quan
m/z
: 58.19
Total Area: 80927
Peak Area: 80927
RT: 2.87 min (2.86)
TAmount: 20.000 ng/mL
Amount: 22.697 ng/mL
Methadone-d3
Quan
m/z
: 268.14
Total Area: 5496688
Peak Area: 5496688
RT: 2.95min (2.94)
Amount: 1.000
Methadone
Quan
m/z
: 265.13
Total Area: 436828
Peak Area: 436828
RT: 2.94min (2.94)
TAmount: 20.000 ng/mL
Amount: 20.943 ng/mL
Propoxyphene-d5
Quan
m/z
: 271.30
TotalArea: 1188454
Peak Area: 1188454
RT: 2.85min (2.85)
Amount: 1.000
EDDP
Quan
m/z
: 234.08
Total Area: 367529
Peak Area: 367529
RT: 2.35 min (2.34)
TAmount: 20.000 ng/mL
Amount: 20.321 ng/mL
Meperidine-d4
Quan
m/z
: 224.20
Total Area: 3159582
Peak Area: 3159582
RT: 1.56min (1.55)
Amount: 1.000
Figure 10. SRM chromatograms of six synthetic opiates in urine at 20 ng/mL